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Synthesis and powder XRD characterization of Al2-xInx(WO4)3 solid solutions

Identifieur interne : 004A42 ( Main/Repository ); précédent : 004A41; suivant : 004A43

Synthesis and powder XRD characterization of Al2-xInx(WO4)3 solid solutions

Auteurs : RBID : Pascal:09-0249424

Descripteurs français

Pascal (Inist)
- Technologie poudre, Diffraction RX, Croissance cristalline, Optimisation, Structure état solide, Structure solution, Paramètre cristallin, Structure cristalline, Indium, Réaction état solide, Tungstate d'aluminium, Solution solide, Polycristal, Monocristal, Al2(WO4)3, In, 8120E.

English descriptors

KwdEn :
- Aluminium tungstates, Crystal growth, Crystal structure, Indium, Lattice parameters, Monocrystals, Optimization, Polycrystals, Powder technology, Solid solutions, Solid state reaction, Solid structure, Solution structure, XRD.

Abstract

The synthesis of polycrystalline materials as well as the conditions for single crystals growth of solid solution compounds with general formula Al_2-xIn_x(WO₄)₃ have been investigated and optimized. The solid solutions structure and the changes in the lattice parameters corresponding to the indium concentration in the materials have been established. The single crystals growth has shown that the indium effective distribution coefficients depend on the initial indium concentration and they strongly differ from unity.

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Le document en format XML

<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Synthesis and powder XRD characterization of Al<sub>2-x</sub>
In<sub>x</sub>
(WO<sub>4</sub>
)<sub>3</sub>
 solid solutions</title>
<author><name sortKey="Tzvetkov, Peter" uniqKey="Tzvetkov P">Peter Tzvetkov</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences</s1>
<s2>1113 Sofia</s2>
<s3>BGR</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>Bulgarie</country>
<placeName><settlement type="city">Sofia</settlement>
<region nuts="2">Sofia-ville (oblast)</region>
</placeName>
</affiliation>
</author>
<author><name sortKey="Ivanova, Donka" uniqKey="Ivanova D">Donka Ivanova</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences</s1>
<s2>1113 Sofia</s2>
<s3>BGR</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>Bulgarie</country>
<placeName><settlement type="city">Sofia</settlement>
<region nuts="2">Sofia-ville (oblast)</region>
</placeName>
</affiliation>
</author>
<author><name sortKey="Kovacheva, Daniela" uniqKey="Kovacheva D">Daniela Kovacheva</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences</s1>
<s2>1113 Sofia</s2>
<s3>BGR</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>Bulgarie</country>
<placeName><settlement type="city">Sofia</settlement>
<region nuts="2">Sofia-ville (oblast)</region>
</placeName>
</affiliation>
</author>
<author><name sortKey="Nikolov, Velin" uniqKey="Nikolov V">Velin Nikolov</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences</s1>
<s2>1113 Sofia</s2>
<s3>BGR</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>Bulgarie</country>
<placeName><settlement type="city">Sofia</settlement>
<region nuts="2">Sofia-ville (oblast)</region>
</placeName>
</affiliation>
</author>
</titleStmt>
<publicationStmt><idno type="inist">09-0249424</idno>
<date when="2009">2009</date>
<idno type="stanalyst">PASCAL 09-0249424 INIST</idno>
<idno type="RBID">Pascal:09-0249424</idno>
<idno type="wicri:Area/Main/Corpus">005585</idno>
<idno type="wicri:Area/Main/Repository">004A42</idno>
</publicationStmt>
<seriesStmt><idno type="ISSN">0925-8388</idno>
<title level="j" type="abbreviated">J. alloys compd.</title>
<title level="j" type="main">Journal of alloys and compounds</title>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aluminium tungstates</term>
<term>Crystal growth</term>
<term>Crystal structure</term>
<term>Indium</term>
<term>Lattice parameters</term>
<term>Monocrystals</term>
<term>Optimization</term>
<term>Polycrystals</term>
<term>Powder technology</term>
<term>Solid solutions</term>
<term>Solid state reaction</term>
<term>Solid structure</term>
<term>Solution structure</term>
<term>XRD</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Technologie poudre</term>
<term>Diffraction RX</term>
<term>Croissance cristalline</term>
<term>Optimisation</term>
<term>Structure état solide</term>
<term>Structure solution</term>
<term>Paramètre cristallin</term>
<term>Structure cristalline</term>
<term>Indium</term>
<term>Réaction état solide</term>
<term>Tungstate d'aluminium</term>
<term>Solution solide</term>
<term>Polycristal</term>
<term>Monocristal</term>
<term>Al2(WO4)3</term>
<term>In</term>
<term>8120E</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">The synthesis of polycrystalline materials as well as the conditions for single crystals growth of solid solution compounds with general formula Al<sub>2-x</sub>
In<sub>x</sub>
(WO<sub>4</sub>
)<sub>3</sub>
 have been investigated and optimized. The solid solutions structure and the changes in the lattice parameters corresponding to the indium concentration in the materials have been established. The single crystals growth has shown that the indium effective distribution coefficients depend on the initial indium concentration and they strongly differ from unity.</div>
</front>
</TEI>
<inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0925-8388</s0>
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<fA03 i2="1"><s0>J. alloys compd.</s0>
</fA03>
<fA05><s2>470</s2>
</fA05>
<fA06><s2>1-2</s2>
</fA06>
<fA08 i1="01" i2="1" l="ENG"><s1>Synthesis and powder XRD characterization of Al<sub>2-x</sub>
In<sub>x</sub>
(WO<sub>4</sub>
)<sub>3</sub>
 solid solutions</s1>
</fA08>
<fA11 i1="01" i2="1"><s1>TZVETKOV (Peter)</s1>
</fA11>
<fA11 i1="02" i2="1"><s1>IVANOVA (Donka)</s1>
</fA11>
<fA11 i1="03" i2="1"><s1>KOVACHEVA (Daniela)</s1>
</fA11>
<fA11 i1="04" i2="1"><s1>NIKOLOV (Velin)</s1>
</fA11>
<fA14 i1="01"><s1>Institute of General and Inorganic Chemistry, Bulgarian Academy of Sciences</s1>
<s2>1113 Sofia</s2>
<s3>BGR</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>4 aut.</sZ>
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<fA20><s1>492-496</s1>
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<fA21><s1>2009</s1>
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<fA43 i1="01"><s1>INIST</s1>
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<fA44><s0>0000</s0>
<s1>© 2009 INIST-CNRS. All rights reserved.</s1>
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<fA60><s1>P</s1>
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<fA61><s0>A</s0>
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<fA64 i1="01" i2="1"><s0>Journal of alloys and compounds</s0>
</fA64>
<fA66 i1="01"><s0>CHE</s0>
</fA66>
<fC01 i1="01" l="ENG"><s0>The synthesis of polycrystalline materials as well as the conditions for single crystals growth of solid solution compounds with general formula Al<sub>2-x</sub>
In<sub>x</sub>
(WO<sub>4</sub>
)<sub>3</sub>
 have been investigated and optimized. The solid solutions structure and the changes in the lattice parameters corresponding to the indium concentration in the materials have been established. The single crystals growth has shown that the indium effective distribution coefficients depend on the initial indium concentration and they strongly differ from unity.</s0>
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<fC02 i1="02" i2="3"><s0>001B80A20</s0>
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<fC03 i1="01" i2="3" l="FRE"><s0>Technologie poudre</s0>
<s5>01</s5>
</fC03>
<fC03 i1="01" i2="3" l="ENG"><s0>Powder technology</s0>
<s5>01</s5>
</fC03>
<fC03 i1="02" i2="3" l="FRE"><s0>Diffraction RX</s0>
<s5>02</s5>
</fC03>
<fC03 i1="02" i2="3" l="ENG"><s0>XRD</s0>
<s5>02</s5>
</fC03>
<fC03 i1="03" i2="3" l="FRE"><s0>Croissance cristalline</s0>
<s5>03</s5>
</fC03>
<fC03 i1="03" i2="3" l="ENG"><s0>Crystal growth</s0>
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<s5>05</s5>
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<fC03 i1="05" i2="3" l="ENG"><s0>Solid structure</s0>
<s5>05</s5>
</fC03>
<fC03 i1="06" i2="X" l="FRE"><s0>Structure solution</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="ENG"><s0>Solution structure</s0>
<s5>06</s5>
</fC03>
<fC03 i1="06" i2="X" l="SPA"><s0>Estructura solución</s0>
<s5>06</s5>
</fC03>
<fC03 i1="07" i2="3" l="FRE"><s0>Paramètre cristallin</s0>
<s5>07</s5>
</fC03>
<fC03 i1="07" i2="3" l="ENG"><s0>Lattice parameters</s0>
<s5>07</s5>
</fC03>
<fC03 i1="08" i2="3" l="FRE"><s0>Structure cristalline</s0>
<s5>08</s5>
</fC03>
<fC03 i1="08" i2="3" l="ENG"><s0>Crystal structure</s0>
<s5>08</s5>
</fC03>
<fC03 i1="09" i2="3" l="FRE"><s0>Indium</s0>
<s2>NC</s2>
<s5>09</s5>
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<fC03 i1="09" i2="3" l="ENG"><s0>Indium</s0>
<s2>NC</s2>
<s5>09</s5>
</fC03>
<fC03 i1="10" i2="X" l="FRE"><s0>Réaction état solide</s0>
<s5>10</s5>
</fC03>
<fC03 i1="10" i2="X" l="ENG"><s0>Solid state reaction</s0>
<s5>10</s5>
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<s5>10</s5>
</fC03>
<fC03 i1="11" i2="3" l="FRE"><s0>Tungstate d'aluminium</s0>
<s2>NK</s2>
<s5>15</s5>
</fC03>
<fC03 i1="11" i2="3" l="ENG"><s0>Aluminium tungstates</s0>
<s2>NK</s2>
<s5>15</s5>
</fC03>
<fC03 i1="12" i2="3" l="FRE"><s0>Solution solide</s0>
<s5>16</s5>
</fC03>
<fC03 i1="12" i2="3" l="ENG"><s0>Solid solutions</s0>
<s5>16</s5>
</fC03>
<fC03 i1="13" i2="3" l="FRE"><s0>Polycristal</s0>
<s5>17</s5>
</fC03>
<fC03 i1="13" i2="3" l="ENG"><s0>Polycrystals</s0>
<s5>17</s5>
</fC03>
<fC03 i1="14" i2="3" l="FRE"><s0>Monocristal</s0>
<s5>18</s5>
</fC03>
<fC03 i1="14" i2="3" l="ENG"><s0>Monocrystals</s0>
<s5>18</s5>
</fC03>
<fC03 i1="15" i2="3" l="FRE"><s0>Al2(WO4)3</s0>
<s4>INC</s4>
<s5>46</s5>
</fC03>
<fC03 i1="16" i2="3" l="FRE"><s0>In</s0>
<s4>INC</s4>
<s5>47</s5>
</fC03>
<fC03 i1="17" i2="3" l="FRE"><s0>8120E</s0>
<s4>INC</s4>
<s5>71</s5>
</fC03>
<fN21><s1>187</s1>
</fN21>
<fN44 i1="01"><s1>OTO</s1>
</fN44>
<fN82><s1>OTO</s1>
</fN82>
</pA>
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Synthesis and powder XRD characterization of Al2-xInx(WO4)3 solid solutions

Synthesis and powder XRD characterization of Al2-xInx(WO4)3 solid solutions

Descripteurs français

English descriptors

Abstract

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Links to Exploration step

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Pour manipuler ce document sous Unix (Dilib)

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